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- W2134225145 abstract "The aging behavior of an epoxy adhesive (DGEBA and DETA) in the bulk surface region and in the contact region to metal substrates (Au, Cu) is studied locally. Therefore, the chemical depth profile during aging is recorded with FTIR microscopy on sample surfaces prepared with low angle microtomy. Two environmental conditions are applied at 60°C for up to 500 days to separate the role of temperature and humidity in aging. Quantitative evaluation of the IR spectra provides the following results: in the bulk surface region, three aging mechanisms form a gradient region of more than 200 μm. Their intensity and depth profile depend on the environmental conditions. Epoxy-metal contacts are unaffected under dry conditions. Humidity is needed to form a 50 μm thick region where the copper substrate accelerates aging. Based on the experimental results, chemical aging mechanisms are discussed." @default.
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- W2134225145 date "2008-04-29" @default.
- W2134225145 modified "2023-09-27" @default.
- W2134225145 title "Chemical Aging in Epoxies: A Local Study of the Interphases to Air and to Metals" @default.
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- W2134225145 doi "https://doi.org/10.1080/00218460802004360" @default.
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