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• W2134285405 startingPage "267" @default.
• W2134285405 abstract "One-, two- and three-bond carbon-13; proton scalar spin-spin coupling constants (1JC,H, 2JC,H,3JC,H) have been determined for a series of hydantoin- and 2-thiohydantoin derivatives in DMSO-d6 solution using one- and two-dimensional NMR techniques. Simultaneous consideration of several coupling data allowed reliable estimates to be deduced for the ring dihedrals equivalent to the ϕ, ψ and ω angles in peptides. These data are in support of a quasi-planar geometry for the hydantoin ring in solution in close agreement with previous results obtained for the solid state. Rotamer population distributions around the C5C1′ bond have been determined for some 5-substituted derivatives. The existence of four-bond couplings between amide NH protons in 1,3-positions of the imidazolidine ring has been demonstrated for the first time." @default.
• W2134285405 created "2016-06-24" @default.
• W2134285405 creator A5011320175 @default.
• W2134285405 creator A5041318802 @default.
• W2134285405 creator A5052880988 @default.
• W2134285405 date "1998-02-01" @default.
• W2134285405 modified "2023-10-17" @default.
• W2134285405 title "Structural analysis of hydantoins and 2-thiohydantoins in solution using 13C, 1H NMR coupling constants" @default.
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• W2134285405 doi "https://doi.org/10.1016/s0022-2860(97)00357-8" @default.
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