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- W2134906110 abstract "Abstract Seven discrete sugar‐pendant diamines were complexed to the {M(CO) 3 } + ( 99m Tc/Re) core: 1,3‐diamino‐2‐propyl β‐ D ‐glucopyranoside ( L 1 ), 1,3‐diamino‐2‐propyl β‐ D ‐xylopyranoside ( L 2 ), 1,3‐diamino‐2‐propyl α‐ D ‐mannopyranoside ( L 3 ), 1,3‐diamino‐2‐propyl α‐ D ‐galactopyranoside ( L 4 ), 1,3‐diamino‐2‐propyl β‐ D ‐galactopyranoside ( L 5 ), 1,3‐diamino‐2‐propyl β‐(α‐ D ‐glucopyranosyl‐(1,4)‐ D ‐glucopyranoside) ( L 6 ), and bis(aminomethyl)bis[(β‐ D ‐glucopyranosyloxy)methyl]methane ( L 7 ). The Re complexes [Re( L 1 – L 7 )(Br)(CO) 3 ] were characterized by 1 H and 13 C 1D/2D NMR spectroscopy which confirmed the pendant nature of the carbohydrate moieties in solution. Additional characterization was provided by IR spectroscopy, elemental analysis, and mass spectrometry. Two analogues, [Re( L 2 )(CO) 3 Br] and [Re( L 3 )(CO) 3 Br], were characterized in the solid state by X‐ray crystallography and represent the first reported structures of Re organometallic carbohydrate compounds. Conductivity measurements in H 2 O established that the complexes exist as [Re( L 1 – L 7 )(H 2 O)(CO) 3 ]Br in aqueous conditions. Radiolabelling of L 1 – L 7 with [ 99m Tc(H 2 O) 3 (CO) 3 ] + afforded in high yield compounds of identical character to the Re analogues. The radiolabelled compounds were determined to exhibit high in vitro stability towards ligand exchange in the presence of an excess of either cysteine or histidine over a 24 h period." @default.
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- W2134906110 date "2004-12-15" @default.
- W2134906110 modified "2023-10-17" @default.
- W2134906110 title "Novel Carbohydrate‐Appended Metal Complexes for Potential Use in Molecular Imaging" @default.
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- W2134906110 doi "https://doi.org/10.1002/chem.200400719" @default.
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