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- W2135133061 abstract "Reaktionen von RMgX- bzw. RMgX · 2L-Verbindungen führen in Tetrahydrofuran mit KYCN über Halogenid-Pseudohalogenid-Austauschreaktionen zu RMgNCY-Reaktionslösungen (R = Alkyl- oder Arylgruppen; X Cl, Br, I; L O-Donoren; Y S, Se), aus denen kristalline Verbindungen des Typs RMgNCY · 2 THF isolierbar sind. Die dargestellten Verbindungen werden durch IR-Absorptionsspektren, konzentrationsabhängige Elektrolytleitfähigkeitsmessungen und ihr Reaktionsverhalten im Vergleich zu „klassischen Grignardverbindungen”︁ näher charakterisiert. Cyanates and their Reactive Behaviour. XLIII. Synthesis and Properties of Organomagnesium Thiocyanate and Selenocyanate Compounds RMgX and RMgX · 2 L compounds react with KYCN in tetrahydrofurane via halide pseudohalide exchange reactions to give RMgNCY solutions (R = alkyl or aryl groups; X Cl, Br, I; L O-donors; Y S, Se), from which compounds of the type RMgNCY · 2 THF have been isolated in a crystalline form. The prepared compounds are characterized by analytical data, IR absorption spectra, concentration dependent conductivity measurements and reactive behaviour in relation to classic Grignard reagents." @default.
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- W2135133061 date "1989-10-01" @default.
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- W2135133061 title "�ber Cyanatverbindungen und deren reaktives Verhalten. XLIII. Darstellung und Eigenschaften von Organomagnesiumthiocyanat- und -selenocyanat-Verbindungen" @default.
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- W2135133061 doi "https://doi.org/10.1002/zaac.19895770106" @default.
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