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- W2135253457 abstract "A novel layered lead titanate with the approximate composition PbTiO2(CO3)0.3 (NO3)0.35(OH) has been synthesized hydrothermally under acidic conditions. The structure has been solved and refined from X-ray and neutron powder diffraction data in the space group P -3 1 m, with cell dimensions a = 5.1787(5) Å and c = 8.5222(7) Å. The titanate layers possess a gibbsite-like structure: lead cations and oxyanions such as carbonate and nitrate are included between the layers. Upon heating the solid loses water, carbon dioxide and nitrogen dioxide and converts via a poorly crystalline intermediate phase to the perovskite PbTiO3. The conversion is complete by 550°C; continued heating results in an increase in crystallinity." @default.
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- W2135253457 date "2001-07-01" @default.
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- W2135253457 title "The preparation of a novel layered lead titanate and its conversion to the perovskite lead titanate PbTiO3" @default.
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- W2135253457 doi "https://doi.org/10.1016/s0025-5408(01)00663-8" @default.
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