Matches in SemOpenAlex for { <https://semopenalex.org/work/W2135453485> ?p ?o ?g. }
Showing items 1 to 85 of
85
with 100 items per page.
- W2135453485 endingPage "528" @default.
- W2135453485 startingPage "522" @default.
- W2135453485 abstract "CE with indirect UV detection was used for the simultaneous determination of lithium, magnesium, calcium, creatinine, carnitine, and a number of amino acids in human serum. The target analytes, positively charged under acidic electrolyte conditions, were separated with positive separation voltage polarity using 10 mM 4-methylbenzylamine, 4.5 mM citric acid, 25% (v/v) methanol at pH 4.05 as background electrolyte providing optimal separation. When analyzing real samples, however, some peaks were broadened due to essentially destacking conditions. In order to maintain the separation efficiency and also enhance the detection sensitivity, transient isotachophoresis (tITP) sample stacking was applied and yielded theoretical plate numbers in the range from 160,000 (arginine) to 350,000 (creatinine). The limit of detection values with tITP preconcentration were 0.11-0.26 mg L(-1) for metal cations, 1.0 mg L(-1) for creatinine, and 1.3-3.9 mg L(-1) for histidine, lysine, arginine, and ornithine. The method precision for peak areas was from 0.4 to 5.0% relative standard deviation using the matrix sodium as internal standard. The accuracy of the developed tITP-CZE system was verified by consistent results for Li+, Mg2+, Ca2+, and creatinine obtained on analyzing two serum certified reference materials. The only sample preparation required was ultrafiltration and acidification (to release protein-bound alkaline earths), and working ranges for individual analytes corresponded well to clinical concentration ranges." @default.
- W2135453485 created "2016-06-24" @default.
- W2135453485 creator A5025933427 @default.
- W2135453485 creator A5027918582 @default.
- W2135453485 creator A5035718082 @default.
- W2135453485 date "2005-04-01" @default.
- W2135453485 modified "2023-10-10" @default.
- W2135453485 title "Simultaneous determination of metal ions, amino acids, and other small biogenic molecules in human serum by capillary zone electrophoresis with transient isotachophoretic preconcentration" @default.
- W2135453485 cites W1965668642 @default.
- W2135453485 cites W1975252428 @default.
- W2135453485 cites W1978271257 @default.
- W2135453485 cites W1981081870 @default.
- W2135453485 cites W1987009344 @default.
- W2135453485 cites W1989088380 @default.
- W2135453485 cites W1993367376 @default.
- W2135453485 cites W2009675810 @default.
- W2135453485 cites W2014276977 @default.
- W2135453485 cites W2022185939 @default.
- W2135453485 cites W2028802467 @default.
- W2135453485 cites W2049412456 @default.
- W2135453485 cites W2058845334 @default.
- W2135453485 cites W2069313678 @default.
- W2135453485 cites W2094808471 @default.
- W2135453485 cites W2119075253 @default.
- W2135453485 cites W2140761094 @default.
- W2135453485 cites W2490044118 @default.
- W2135453485 cites W4300855835 @default.
- W2135453485 doi "https://doi.org/10.1002/jssc.200400070" @default.
- W2135453485 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/15881081" @default.
- W2135453485 hasPublicationYear "2005" @default.
- W2135453485 type Work @default.
- W2135453485 sameAs 2135453485 @default.
- W2135453485 citedByCount "34" @default.
- W2135453485 countsByYear W21354534852012 @default.
- W2135453485 countsByYear W21354534852013 @default.
- W2135453485 countsByYear W21354534852019 @default.
- W2135453485 countsByYear W21354534852020 @default.
- W2135453485 crossrefType "journal-article" @default.
- W2135453485 hasAuthorship W2135453485A5025933427 @default.
- W2135453485 hasAuthorship W2135453485A5027918582 @default.
- W2135453485 hasAuthorship W2135453485A5035718082 @default.
- W2135453485 hasConcept C100859065 @default.
- W2135453485 hasConcept C10390740 @default.
- W2135453485 hasConcept C113196181 @default.
- W2135453485 hasConcept C119128265 @default.
- W2135453485 hasConcept C147789679 @default.
- W2135453485 hasConcept C17525397 @default.
- W2135453485 hasConcept C185592680 @default.
- W2135453485 hasConcept C186293402 @default.
- W2135453485 hasConcept C2900643 @default.
- W2135453485 hasConcept C43617362 @default.
- W2135453485 hasConcept C68801617 @default.
- W2135453485 hasConceptScore W2135453485C100859065 @default.
- W2135453485 hasConceptScore W2135453485C10390740 @default.
- W2135453485 hasConceptScore W2135453485C113196181 @default.
- W2135453485 hasConceptScore W2135453485C119128265 @default.
- W2135453485 hasConceptScore W2135453485C147789679 @default.
- W2135453485 hasConceptScore W2135453485C17525397 @default.
- W2135453485 hasConceptScore W2135453485C185592680 @default.
- W2135453485 hasConceptScore W2135453485C186293402 @default.
- W2135453485 hasConceptScore W2135453485C2900643 @default.
- W2135453485 hasConceptScore W2135453485C43617362 @default.
- W2135453485 hasConceptScore W2135453485C68801617 @default.
- W2135453485 hasIssue "6" @default.
- W2135453485 hasLocation W21354534851 @default.
- W2135453485 hasLocation W21354534852 @default.
- W2135453485 hasOpenAccess W2135453485 @default.
- W2135453485 hasPrimaryLocation W21354534851 @default.
- W2135453485 hasRelatedWork W1983052253 @default.
- W2135453485 hasRelatedWork W2013312445 @default.
- W2135453485 hasRelatedWork W2027234809 @default.
- W2135453485 hasRelatedWork W2034504378 @default.
- W2135453485 hasRelatedWork W2040411552 @default.
- W2135453485 hasRelatedWork W2083314461 @default.
- W2135453485 hasRelatedWork W2089621476 @default.
- W2135453485 hasRelatedWork W2417228964 @default.
- W2135453485 hasRelatedWork W3011010783 @default.
- W2135453485 hasRelatedWork W4245504503 @default.
- W2135453485 hasVolume "28" @default.
- W2135453485 isParatext "false" @default.
- W2135453485 isRetracted "false" @default.
- W2135453485 magId "2135453485" @default.
- W2135453485 workType "article" @default.