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- W2135562894 abstract "Abstract Five imidazolium‐based materials have been synthesised and used for the first time as palladium scavengers. Radical reactions of suitable bis‐vinylimidazolium salts led to a series of insoluble materials through homo‐polymerisation, immobilisation with a 3‐mercaptopropyl‐modified silica gel or co‐polymerisation with ethylene glycol dimethylacrylate. These materials were screened as palladium scavengers with a set of palladium(0) and palladium(II) compounds in different solvents and at different starting amounts of palladium. In many cases, residual amounts of palladium were lower than 5 ppm, as requested for the manufacture of active pharmaceutical ingredients and fine chemicals. The application of one of these materials as a palladium scavenger in a Suzuki coupling reaction resulted in a 29‐fold abatement of the palladium content in the final product with respect to the control reaction." @default.
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- W2135562894 date "2014-01-23" @default.
- W2135562894 modified "2023-10-18" @default.
- W2135562894 title "Cross-Linked Imidazolium Salts as Scavengers for Palladium" @default.
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- W2135562894 doi "https://doi.org/10.1002/cplu.201300361" @default.
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