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- W2135694249 abstract "α-Fluoro-α,β-unsaturated ketones were prepared from trifluoromethyl ketones via a sequence involving Mg metal promoted successive double defluorination. Trifluoromethyl ketones were transformed to β,β-difluoroenol silyl ethers which were then coupled with aldehydes and ketones to β-hydroxy-α,α-difluoroketones. A second Mg-promoted defluorination of the hydroxyketones followed by acid-catalyzed hydrolysis of γ-hydroxy-β-fluoroenol silyl ethers provided α-fluoro-α,β-unsaturated ketones as a final product." @default.
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- W2135694249 date "2002-08-01" @default.
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- W2135694249 title "A new sequential defluorination route to α-fluoro-α,β-unsaturated ketones from trifluoromethyl ketones" @default.
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- W2135694249 doi "https://doi.org/10.1016/s0040-4039(02)01343-6" @default.
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