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- W2135877413 abstract "1H and 13C chemical shift assignment of the anhydroglucose units (AGUs) that comprise cellulose acetate with the total degree of substitution of 2.33 was performed by a combination of two-dimensional NMR spectra obtained from COSY, TOCSY, HSQC–TOCSY, and HSQC experiments. In the TOCSY spectra, there are 13 kinds of correlation networks for the H1 to H6′ atoms of AGU; each 1H resonance of the 13 AGUs was assigned from the changes in the intensities of the 1H resonances with TOCSY spin-lock time during the TOCSY experiments. The ring 13C resonances were assigned via analysis of HSQC spectra. Comparison of the shift data enabled the assignment of the 13 AGUs as three types of 2,3,6-tri-acetylated, one type of 2-mono-, 3-mono-, 6-mono-, 2,3-di-, 2,6-di-, and 3,6-di-acetylated AGU, and unsubstituted AGU, and three types of AGUs located in end units. These shift data will be useful for characterizing the molecular structures of cellulose derivatives as well as cellulose acetate (CA)." @default.
- W2135877413 created "2016-06-24" @default.
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- W2135877413 date "1981-03-01" @default.
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- W2135877413 title "Partial acetylation of β-l(and l)-arabinose and methyl β-l(and l)-arabino-pyranoside, and related 13C-n.m.r. studies" @default.
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- W2135877413 doi "https://doi.org/10.1016/s0008-6215(00)85259-3" @default.
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