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• W2136546330 abstract "During the solution reaction of NaBH4/(NH4)2SO4 in tetraglyme to form borazine, polymeric aminoborane (NH2BH2)x has been isolated as a white powder. The powder was characterized by thermal gravimetric analysis/differential scanning calorimetry, infrared and mass spectroscopies, and powder X-ray diffraction. Solid-state 15N and 11B nuclear magnetic resonance firmly proved that the chain-like poly(aminoborane) evolved a partially condensed B3N3 ring structure by dehydrogenative condensation between chains at 200 °C. Pyrolysis of the polymer in a nitrogen stream up to 1400 °C led to a 75% yield of hexagonal boron nitride with an interlayer spacing of 3.37 Å. Copyright © 1999 John Wiley & Sons, Ltd." @default.
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• W2136546330 date "1999-12-01" @default.
• W2136546330 modified "2023-10-16" @default.
• W2136546330 title "Synthesis and characterization of poly(aminoborane) as a new boron nitride precursor" @default.
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• W2136546330 doi "https://doi.org/10.1002/(sici)1099-1581(199912)10:12<702::aid-pat931>3.0.co;2-q" @default.
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