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- W2137163618 abstract "MoN nanoparticles in a size range around 50 nm were obtained on CNTs support via a novel carbothermal reduction nitridation (CRN). For the first time, a common (NH4)6Mo7O24·4H2O can be used as a Mo source to prepare MoN nanoparticles. A Mo-containing precursor was in a first step carburized and was reduced to a MoOxCy/Mo mixture. During further carbothermal nitridation this mixture-phase was shifted to the MoN phase through either a Mo2C or MoOxNy intermediate. Compared with the conventional NH3-temperature-programmed treatment (TPT) route that produced Mo nitride from MoO2 with rigorous heating method, the CRN route favored the formation of Mo nitride from easily nitridable MoOxCy/Mo, MoOxNy and Mo2C intermediates. The phase structure of the Mo nitride product was greatly dependent on nitridation reaction pathway. The NH3-TPT route yielded cubic Mo2N, while the CRN process produced hexagonal MoN." @default.
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- W2137163618 date "2011-01-01" @default.
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- W2137163618 title "A novel carbothermal reduction nitridation route to MoN nanoparticles on CNTs support" @default.
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- W2137163618 doi "https://doi.org/10.1039/c1jm10833f" @default.
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