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- W2138723903 abstract "Benzoyl radicals are generated directly from (hetero)aromatic aldehydes upon tetrabutylammonium decatungstate ((n-Bu4N)4W10O32), TBADT) photocatalysis under mild conditions. In the presence of α,β-unsaturated esters, ketones and nitriles radical conjugate addition ensues and gives the corresponding β-functionalized aryl alkyl ketones in moderate to good yields (stereoselectively in the case of 3-methylene-2-norbornanone). Due to the mild reaction conditions the presence of various functional groups on the aromatic ring is tolerated (e.g. methyl, methoxy, chloro). The method can be applied to hetero-aromatic aldehydes whether electron-rich (e.g. thiophene-2-carbaldehyde) or electron-poor (e.g. pyridine-3-carbaldehyde)." @default.
- W2138723903 created "2016-06-24" @default.
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- W2138723903 date "2010-01-01" @default.
- W2138723903 modified "2023-10-18" @default.
- W2138723903 title "Benzoyl radicals from (hetero)aromatic aldehydes. Decatungstate photocatalyzed synthesis of substituted aromatic ketones" @default.
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- W2138723903 doi "https://doi.org/10.1039/c0ob00066c" @default.
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