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- W2139471004 abstract "The reactions of the lithiated trialkylsiloxy-cyclopentadienyl ethers (C5H4OSiR3 R3 Et3, Me21Bu, 1Pr3) with TiCl4, ZrCl4, Cp ∗ZrCl3 or CpTiCl3 result in the formation of the respective metallocene dichlorides [(C5H4OSiR3)2TiCl2. (C5H4OSiR3)2ZrCl2, (C5H4OSiR3)(C5H5)TiCl2, (C5H4OSiR3)(C5Me5)ZrCl2)] in moderate to good yields. The reaction of Li(C5H4OSiEt3) with Cp ∗TiCl3 in toluene produced, in addition to the expected complex (C5H4OSiEt3)(C5Me5TiCl2, the hydroxytitanocene dichloride (C5H4OH)(C5Me5)TiCl2 in a yield of 21%. The half-sandwich complex C5H4(OSiMe21Bu)TiCl3 was formed with C5H4(OSiMe21Bu)(SiMe3) and TiCl4." @default.
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- W2139471004 date "1997-10-01" @default.
- W2139471004 modified "2023-09-24" @default.
- W2139471004 title "η5-complexes of cyclopentadienylsilylethers (C5H4OSiR3) and hydroxycyclopentadiene (C5H4OH) with titanium and zirconium chlorides" @default.
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- W2139471004 doi "https://doi.org/10.1016/s0022-328x(97)00325-2" @default.
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