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• W2139849093 abstract "Thermally stimulated depolarization current (TSDC) signals measured in polymers at the glass transition T <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>g</sub> often exhibit intricate shapes that much depend on the thermal history and on the non-stationary condition used during experiments. This peculiar behavior is frequently explained in terms of a physical singularity of the molecular motions. We show that this singularity, i.e. unexpected values for activation energy and pre-exponential factor, obtained around T <sub xmlns:mml=http://www.w3.org/1998/Math/MathML xmlns:xlink=http://www.w3.org/1999/xlink>g</sub> , result from the misuse of the Arrhenius law for treating the experimental data obtained in non-stationary experimental conditions. A simple model using time dependent configurational entropy for the material evolution and using a single Debye relaxation for the dielectric relaxation process is therefore proposed to explain the experimental behavior. The influence of the heating rate and of a non-Debye relaxation on the TSDC signal is also studied and clearly shows that the peculiar behavior of TSDC peaks can originate from the conjugated effects of entropy relaxation and non-Debye response" @default.
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• W2139849093 date "2006-10-01" @default.
• W2139849093 modified "2023-10-18" @default.
• W2139849093 title "An explanation of the peculiar behavior of TSDC peaks at Tg: a simple model of entropy relaxation" @default.
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• W2139849093 doi "https://doi.org/10.1109/tdei.2006.247830" @default.
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