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- W2140367616 abstract "Die Bis(aryloxy)germylene 1-4 und Diaminogermylene 5-10 werden aus GeCl2-Dioxan und lithiierten, ortho-substituierten Phenolen bzw. sterisch gehinderten Aminen (1:2) erhalten. Verbindungen R(Me3Si)NGeOtBu (13-15) entstehen dabei, wenn die Amine mit tert-Butyllithium in n-Hexan/THF lithiiert werden. Dilithiierte Ethylendiamine geben die Diazagerma(II)cyclopentane 16 und 17. Die Amino(halogen)germylene 19 bzw. 20 werden aus GeX2-Dioxan (X = Cl, Br) mit lithiierten (2,6-Dialkylphenyl)(trimethylsilyl)aminen (1:1) erhalten. Synthesis and Isolation of New Germanium(II) Compounds and of Free Germylenes The bis(aryloxy)germylenes 1-4 and the diaminogermylenes 5-10 are obtained from GeCl2-dioxane and lithiated, ortho-substituted phenols and sterically hindered amines (1:2), resp. Compounds R(Me3Si)NGeOtBu (13-15) are formed if the amines are lithiated with tert-butyllithium in n-hexane/THF. Dilithiated ethylenediamines lead to the diazagerma(II)cyclopentanes 16 and 17. The amino(halo)germylenes 19 and 20 are obtained from GeX2-dioxane (X = Cl, Br) and lithiated (2,6-dialkylphenyl)trimethylsilyl)amines (1:1)." @default.
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- W2140367616 date "1985-05-01" @default.
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- W2140367616 title "Synthese und Isolierung neuer Germanium(II)‐Verbindungen und freier Germylene" @default.
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- W2140367616 doi "https://doi.org/10.1002/cber.19851180525" @default.
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