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- W2140462235 abstract "Reductive Co Alkylation of Heptamethyl Cobyrinate with the Methylthiomalonate (S)-Methyl 3-Bromo-2-[(ethylthio)carbonyl]-2-methylpropanoate The methylthiomalonate(−)-(S)-Methyl 3-bromo-2-[(ethylthio)carbonyl]-2-methylpropanoate(5a)was prepared from dimethyl methylmalonate in five steps via the stereospecific cleavage of the (pro-S)-ester group of 1 with pig-liver esterase in an overall yield of 26.5% (Scheme 4a). Reductive Co alkylation of heptamethyl Coβ-perchlorato cob (II)yrinate (8) with 5a by electrosynthesis lead to the alkylcobalt complex 9a in 40% yield (Scheme 4b). The O2-dependent reactions of the methyhnalonyl fragment produced by photolysis of 9a and its deuterated derivative 9c are reported (Scheme 5)." @default.
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- W2140462235 date "1990-09-19" @default.
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- W2140462235 title "Reduktive Co-Alkylierung von Heptamethyl-cobyrinat mit dem Methylthiomalonat (<i>S</i>)-Methyl-3-bromo-2-[(ethylthio) carbonyl]-2-methylpropanoat" @default.
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- W2140462235 doi "https://doi.org/10.1002/hlca.19900730611" @default.
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