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• W2141566605 startingPage "831" @default.
• W2141566605 abstract "Abstract The 9‐methoxy‐9‐borabicyclo[3.3.1]nonane‐based B ‐alkyl Suzuki–Miyaura cross‐coupling reaction (the 9‐MeO‐9‐BBN variant) has been efficiently performed by using the catalyst consisting of Pd(OAc) 2 and a hemilabile P,O‐ligand, Aphos‐Y, under mild reaction conditions (K 3 PO 4 · 3H 2 O, THF/H 2 O, room. temp.). For applications in the total synthesis of structurally complex natural products, the Johnson protocol commonly uses two ligands (dppf and Ph 3 As) and two organic solvents (THF and DMF). In contrast, the new version reported here employs one ligand (Aphos‐Y) and one organic solvent (THF). Moreover, the broad substrate scope and the excellent functional group tolerance of the Pd(OAc) 2 –Aphos‐Y catalyst have been demonstrated, providing a reliable and simple synthetic tool for fragment coupling in total synthesis through formation of a C(sp 3 )–C(sp 2 ) bond." @default.
• W2141566605 created "2016-06-24" @default.
• W2141566605 creator A5018641849 @default.
• W2141566605 creator A5079048867 @default.
• W2141566605 date "2013-01-02" @default.
• W2141566605 modified "2023-10-10" @default.
• W2141566605 title "An Efficient and Reliable Catalyst System Using Hemilabile Aphos for<i>B</i>-Alkyl Suzuki-Miyaura Cross-Coupling Reaction with Alkenyl Halides" @default.
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• W2141566605 doi "https://doi.org/10.1002/ejoc.201201602" @default.
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