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• W2141656206 abstract "Molybdenum concentration and δ98/95Mo values for NIST SRM 610 and 612 (solid glass), NIST SRM 3134 (lot 891307; liquid) and IAPSO seawater reference material are presented based on comparative measurements by MC-ICP-MS performed in laboratories at the Universities of Bern and Oxford. NIST SRM 3134 and NIST SRM 610 and 612 were found to have identical and homogeneous 98Mo/95Mo ratios at a test portion mass of 0.02 g. We suggest, therefore, that NIST SRM 3134 should be used as reference for the δ–Mo notation and to employ NIST SRM 610 or 612 as solid silicate secondary measurement standards, in the absence of an isotopically homogeneous solid geological reference material for Mo. The δ98/95MoJMC Bern composition (Johnson Matthey ICP standard solution, lot 602332B as reference) of NIST SRM 3134 was 0.25 ± 0.09‰ (2s). Based on five new values, we determined more precisely the mean open ocean δ98/95MoSRM 3134 value of 2.09 ± 0.07‰, which equals the value of δ98/95MoJMC Bern of 2.34 ± 0.07‰. We also refined the Mo concentration data for NIST SRM 610 to 412 ± 9 μg g−1 (2s) and NIST SRM 612 to 6.4 ± 0.7 μg g−1 by isotope dilution. We propose these concentration data as new working values, which allow for more accurate in situ Mo determination using laser ablation ICP-MS or SIMS. Les concentrations en molybdène ainsi que les valeurs de δ98/95Mo pour les matériaux de référence NIST SRM 610 et 612 (verre solide), NIST SRM 3134 (lot 891307; liquide) et IAPSO (eau de mer) sont présentées sur la base de mesures comparatives obtenues par MC-ICP-MS et effectuées dans les laboratoires des Universités de Berne et d’Oxford. Pour NIST SRM 3134 et NIST SRM 610 et 612 les rapports 98Mo/95Mo mesurés sont identiques et homogènes pour une portion d’échantillon-test de 0.02 g. Par conséquent, nous suggérons que le NIST SRM 3134 devrait être utilisé comme référence pour la notation δ-Mo, et d’employer les solides silicatés NIST SRM 610 ou 612 comme mesures standards secondaires, en l’absence d’un matériau géologique solide de référence isotopiquement homogène pour Mo. La valeur du δ98/95MoJMC Bern (solution standard Johnson Matthey ICP, lot de référence 602332B) du NIST SRM 3134 était de 0.25 ± 0.09‰ (2s). Sur la base de cinq nouvelles valeurs, nous avons déterminé plus précisément la valeur moyenne de δ98/95MoSRM 3134 pleine mer qui est de 2.09 ± 0.07‰, et qui équivaut de la valeur de δ98/95MoJMC Bern de 2.34 ± 0.07‰. Nous avons également affiné les valeurs de la concentration du Mo pour le NIST SRM 610 à 412 ± 9 μg g−1 (2s) et le NIST SRM 612 à 6.4 ± 0.7 μg g−1 par la méthode de dilution isotopique. Nous proposons ces concentrations comme nouvelles valeurs de travail, permettant la détermination plus précise du Mo in situ par les techniques LA-ICP-MS ou SIMS." @default.
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• W2141656206 date "2012-05-04" @default.
• W2141656206 modified "2023-10-16" @default.
• W2141656206 title "δ98/95Mo values and Molybdenum Concentration Data for NIST SRM 610, 612 and 3134: Towards a Common Protocol for Reporting Mo Data" @default.
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• W2141656206 doi "https://doi.org/10.1111/j.1751-908x.2012.00160.x" @default.
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