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• W2142051645 abstract "Uranium L III -edge X-ray absorption spectroscopy is often used to probe the oxidation state and coordination of uranium in environmental samples, and micrometre-sized beams can be used to spatially map the distribution of uranium relative to other elements. Here a variety of uranium-containing environmental samples are analyzed at both microbeam and larger beam sizes to determine whether reoxidation of U(IV) occurred. Monomeric U(IV), a recently discovered product of U(VI) reduction by microbes and certain iron-bearing minerals at uranium-contaminated field sites, was found to be reoxidized during microbeam (3 µm × 2 µm) analysis of biomass and sediments containing the species but not at larger beam sizes. Thus, care must be taken when using X-ray microprobes to analyze samples containing monomeric U(IV)." @default.
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• W2142051645 date "2012-11-22" @default.
• W2142051645 modified "2023-10-03" @default.
• W2142051645 title "Beam-induced oxidation of monomeric U(IV) species" @default.
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• W2142051645 doi "https://doi.org/10.1107/s0909049512041763" @default.
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