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- W2142761330 abstract "Abstract The Stille cross‐coupling of allylic and benzyl bromides is shown to proceed efficiently using phosphine‐free dinuclear anionic palladacyclopentadienyl catalysts possessing bridging ( N , O )‐imidate ligands. The type of bridging anion influences the catalytic activity considerably. Halide anions such as chloride, bromide or iodide also influence the catalytic activity but to a far lesser extent than the pseudohalide imidate anions (from succinimide or phthalimide). A Baldwin‐type cooperative effect is seen with 7a using CuI as a co‐catalyst, in the presence of two equivalents of CsF in DMF at 40 °C. In toluene, these additives slow down substrate turnover." @default.
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- W2142761330 date "2006-03-01" @default.
- W2142761330 modified "2023-10-17" @default.
- W2142761330 title "Air‐Stable, Phosphine‐Free Anionic Palladacyclopentadienyl Catalysts: Remarkable Halide and Pseudohalide Effects in Stille Coupling" @default.
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- W2142761330 doi "https://doi.org/10.1002/adsc.200505325" @default.
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