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- W2142802190 abstract "One- and two-dimensional NMR spectroscopy were employed to determine the conformation of 2,3,4,6,2′,3′-hexa-O-acetyl-4-O-α-D-glucopyranosyl-1′,6′-anhydro-β-D-glucopyranose in acetone-d6 solution. Inter-residue interproton distances, H-1–H-4′ and H-1–H-3′, determined by 2D NOE experiments are commensurate with torsional angles ϕ and Ψ of −10° and −20°, and also of 10° and −30°, about the inter-residue glucosidic bond. Computer simulation showed that, within the limits of the experimental error (ca ±0.20 Å) of the interproton distances determined, several sets of ϕ and ψ angles are consistent with the NMR data. These ‘allowed’ conformations are presented in the form of a conformational map." @default.
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- W2142802190 date "1988-05-01" @default.
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- W2142802190 title "Study of disaccharide conformation by one-and two-dimensional NMR spectroscopy: 1,6-anhydro-β-maltose hexaacetate" @default.
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- W2142802190 doi "https://doi.org/10.1002/mrc.1260260506" @default.
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