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- W2143796178 abstract "Abstract New carbohydrate‐based polyesters were prepared from isoidide‐2,5‐dimethanol (extended isoidide, XII ) through melt polymerization with dimethyl esters of terephthalic acid (TA) and furan‐2,5‐dicarboxylic acid (FDCA), yielding semi‐crystalline prepolymers. Subsequent solid‐state post‐condensation (SSPC) gave high molecular weight ( M n =30 kg mol −1 for FDCA) materials, the first examples of high M n , semi‐aromatic homopolyesters containing isohexide derivatives obtained via industrially relevant procedures. NMR spectroscopy showed that the stereo‐configuration of XII was preserved under the applied conditions. The polyesters are thermally stable up to 380 °C. The TA‐ and FDCA‐based polyesters have high T g (105 °C and 94 °C, resp.) and T m (284 °C and 250 °C, resp.) values. Its reactivity, stability, and ability to afford high T g and T m polyesters make XII a promising diol for the synthesis of engineering polymers." @default.
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- W2143796178 date "2014-11-07" @default.
- W2143796178 modified "2023-10-18" @default.
- W2143796178 title "Semi-Aromatic Polyesters Based on a Carbohydrate-Derived Rigid Diol for Engineering Plastics" @default.
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- W2143796178 doi "https://doi.org/10.1002/cssc.201402935" @default.
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