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• W2145159179 abstract "Three tetra-armed cyclens with two kinds of side-arms, 3',5'-difluorobenzyl/4'-methylbenzyl, 3',5'-difluorobenzyl/1'-naphthylmethyl, and 3',5'-difluorobenzyl/9'-anthrylmethyl groups, were prepared by reductive amination of 1,7-bis(3',5'-difluorobenzyl)-1,4,7,10-tetraazacyclododecane and the corresponding aromatic aldehydes in the presence of NaBH(OAc)3. The X-ray structures of the Ag(+) complexes and Ag(+)-ion-induced (1)H NMR spectral changes suggest that (i) the chemical shift changes of the protons at the 2'- and 6'-positions in the 3',5'-difluorobenzyl/4'-methylbenzyl side-arms are dependent on the electron density on the adjacent substituted benzenes, and (ii) in the tetra-armed cyclens with 3',5'-difluorobenzyl/1'-naphthylmethyl and 3',5'-difluorobenzyl/9'-anthrylmethyl groups as side-arms, electron-rich aromatic rings preferentially cover the Ag(+) ions incorporated into the ligand cavities, and 3',5'-difluorobenzyl groups do not participate in the Ag(+) interactions. The log K values were estimated using Ag(+)-ion-induced UV-vis spectral changes." @default.
• W2145159179 created "2016-06-24" @default.
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• W2145159179 date "2013-01-01" @default.
• W2145159179 modified "2023-09-26" @default.
• W2145159179 title "Argentivorous molecules with two kinds of aromatic side-arms: intramolecular competition between side-arms" @default.
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• W2145159179 doi "https://doi.org/10.1039/c3dt00034f" @default.
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