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- W2146202511 abstract "Abstract Abstract. The five‐membered heteroelement cluster THF · Cl 2 In(O t Bu) 3 Sn reacts with the sodium stannate [Na(O t Bu) 3 Sn] 2 to produce either the new oxo‐centered alkoxo cluster ClInO[Sn(O t Bu) 2 ] 3 ( 1 ) (in low yield) or the heteroleptic alkoxo cluster Sn(O t Bu) 3 InCl 3 Na[Sn(O t Bu) 2 ] 2 ( 2 ). X‐ray diffraction analyses reveal that in compound 1 the polycyclic entity is made of three tin atoms which together with a central oxygen atom form a trigonal, almost planar triangle, perpendicular to which a further indium atom is connected through the oxygen atom. The metal atoms thus are arranged in a Sn 3 In pyramid, the edges of which are all saturated by bridging tert ‐butoxy groups. The indium atom has a further chloride ligand. Compound 2 has two trigonal bipyramids as building blocks which are fused together at a six coordinate indium atom. One of the bipyramids is of the type SnO 3 In with tert ‐butyl groups on the oxygen atoms, while the other has the composition InCl 3 Na with chlorine atoms connecting the two metals. The sodium atom in 2 has further contacts to two plus one alkoxide groups which are part of a[Sn(O t Bu) 2 ] 2 dimer disposing of a Sn 2 O 2 central cycle. The hetero element cluster in 2 thus combines three closed entities and its skeleton SnO 3 InCl 3 NaO 2 Sn 2 O 2 consists of three different metallic and two different non‐metallic elements." @default.
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- W2146202511 date "2012-08-01" @default.
- W2146202511 modified "2023-10-09" @default.
- W2146202511 title "Neue molekulare Indium-Zinn-Sauerstoff- und Indium-Zinn-Natrium-Sauerstoff-Chlor-Cluster" @default.
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- W2146202511 doi "https://doi.org/10.1002/zaac.201200273" @default.
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