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• W2146735860 abstract "The 1H NMR spectrum of Pt[η3-CH2C(CH3)CH2](SnCl3)(PhCHCH2) (1), which is complicated by the existence of two isomers, has been interpreted using (195Pt, 1H)-INVERSE, J-resolved, COSY-90 and NOESY two-dimensional methods. The two isomers are shown to be involved in slow exchange processes, and one intermediate in the exchange, Pt[CH2C(CH3)CH2](SnCl3) (4), has been identified and characterized via 1H, 13C, 119Sn and 195Pt spectroscopy. NOESY measurements show that neither 1 nor 4 is involved in an η3 →η1 isomerization, so that 4 must be involved in the dynamics with 1 via loss of a tin-containing fragment, presumably SnCl3−. Uncoordinated PhCHCH2 has been detected in solution and shown to exchange with the complexed PhCHCH2 in both isomers of 1." @default.
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• W2146735860 date "1989-04-01" @default.
• W2146735860 modified "2023-10-16" @default.
• W2146735860 title "Two-dimensional NMR studies of Pt(2-methallyl)(SnCl3)(styrene). Recognition and interpretation of simultaneous exchange processes via1H noesy" @default.
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• W2146735860 doi "https://doi.org/10.1002/mrc.1260270411" @default.
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