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• W2146826384 startingPage "2621" @default.
• W2146826384 abstract "The conformational, configurational behavior and the structure of N-2-(1,4-dioxane)-N′-(p-methylbenzenesulfonyl)-O-(p-methylphenoxy) isourea (1) has been studied using X-ray crystallographic analysis. The endo-anomeric effect controls the population of dioxane ring conformers or anomers but not the configuration interconversion of the imine of the imidoyl moiety. X-Ray analysis of 1 demonstrates that the dioxane ring adopts the chair conformation, that the imidoyl amino group prefers axial conformation and that the tosyl and tolyl groups about the CN bond retain the E configuration. Isourea (1) was synthesized by the thermal decomposition of N′-(p-methylbenzenesulfonyl)-O-(p-methylphenoxy) imidoyl azide in refluxing dioxane." @default.
• W2146826384 created "2016-06-24" @default.
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• W2146826384 creator A5091662551 @default.
• W2146826384 date "2002-03-01" @default.
• W2146826384 modified "2023-10-17" @default.
• W2146826384 title "Experimental demonstration of anomeric effect and structure: X-ray conformational and configurational analysis of N-2-(1,4-dioxane)-N′-(p-methylbenzenesulfonyl)-O-(p-methylphenoxy) isourea" @default.
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• W2146826384 doi "https://doi.org/10.1016/s0040-4020(02)00130-8" @default.
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