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- W2147275737 abstract "Iron(III)5(2′-hydroxyphenyl)-3-(4-X-phenyl)pyrazolinates of the type (C15H12N2OX)3Fe [where X =–H,–Cl,–CH3,–OCH3] have been synthesized by reaction of anhydrous FeCl3 with the sodium salts of pyrazoline in 1 : 3 molar ratio. Their addition complexes with N and P donor ligands [2,2′-bipyridine, 1,10-phenanthroline and triphenylphosphine] were prepared in 1:1 molar ratio. These newly synthesized derivatives have been characterized using elemental analysis (C, H, N and Fe), molecular weight measurement, magnetic moment data, FAB mass, 31P NMR and Mossbauer spectral data. The complexes have been examined for crystalline/amorphous nature through XRD; all complexes are amorphous. Octahedral geometry around iron(III) confirms the presence of three bidentate pyrazoline ligands in iron(III)5(2′-hydroxyphenyl)-3-(4-X-phenyl)pyrazolinates. In addition complexes pyrazoline is monodentate. The bidentate and monodentate behavior of pyrazoline ligands was confirmed by IR spectral data. All the complexes were tested for ..." @default.
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- W2147275737 date "2008-10-13" @default.
- W2147275737 modified "2023-09-24" @default.
- W2147275737 title "Iron(III)5(2′-hydroxyphenyl)-3-(4-X-phenyl)pyrazolinates and their addition complexes with N, P donor ligands: synthesis, spectral and antimicrobial investigations" @default.
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- W2147275737 doi "https://doi.org/10.1080/00958970802044160" @default.
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