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• W2148771519 abstract "Abstract While carboranes with 2 n +2 and 2 n +4 ( n =number of skeletal atoms) skeletal electrons (SE) are widely known, little has been reported on carboranes with odd SE numbers. Electrochemical measurements on two‐cage assemblies, where two C‐phenyl‐ ortho ‐carboranyl groups are linked by a para ‐phenylene or a para ‐tetrafluorophenylene bridge, revealed two well separated and reversible two‐electron reduction waves indicating formation of stable dianions and tetraanions. The salts of the dianions were isolated by reduction with sodium metal and their unusual structures were determined by X‐ray crystallography. The diamagnetic dianions contain two 2 n +3 SE clusters where each cluster has a notably long carborane C–carborane C distance of ca 2.4 Å. The π conjugation within the phenylene bridge plays an important role in the stabilization of these carboranes with odd SE counts." @default.
• W2148771519 created "2016-06-24" @default.
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• W2148771519 date "2014-02-26" @default.
• W2148771519 modified "2023-10-18" @default.
• W2148771519 title "Crystal Structures of the Carborane Dianions [1,4-(PhCB₁₀H₁₀C)₂C₆H₄]²⁻and [1,4-(PhCB₁₀H₁₀C)₂C₆F₄]²⁻and the Stabilizing Role of the<i>para</i>-Phenylene Unit on 2 <i>n</i>+3 Skeletal Electron Clusters" @default.
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• W2148771519 doi "https://doi.org/10.1002/anie.201310718" @default.
• W2148771519 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/4257503" @default.
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