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- W2149256535 abstract "Abstract A catalytic asymmetric intramolecular homologation of simple ketones with α‐diazoesters was firstly accomplished with a chiral N,N′‐dioxide–Sc(OTf) 3 complex. This method provides an efficient access to chiral cyclic α‐aryl/alkyl β‐ketoesters containing an all‐carbon quaternary stereocenter. Under mild conditions, a variety of aryl‐ and alkyl‐substituted ketone groups reacted with α‐diazoester groups smoothly through an intramolecular addition/rearrangement process, producing the β‐ketoesters in high yield and enantiomeric excess." @default.
- W2149256535 created "2016-06-24" @default.
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- W2149256535 creator A5077217676 @default.
- W2149256535 creator A5077232855 @default.
- W2149256535 creator A5089154177 @default.
- W2149256535 date "2014-12-08" @default.
- W2149256535 modified "2023-10-18" @default.
- W2149256535 title "Catalytic Asymmetric Intramolecular Homologation of Ketones with α-Diazoesters: Synthesis of Cyclic α-Aryl/Alkyl β-Ketoesters" @default.
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- W2149256535 doi "https://doi.org/10.1002/anie.201409572" @default.
- W2149256535 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/25488490" @default.
- W2149256535 hasPublicationYear "2014" @default.
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