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- W2149304866 abstract "Calcination and deboronation of [B]-MFI and silanol nest reoccupation of deboronated MFI were studied by variable temperature FT i.r. spectroscopy, X-ray diffraction, and 1 H, 11 B, and 29 Si MAS n.m.r. spectroscopy techniques. Boron loss from the framework upon calcining [B]-MFI was minimized by using an improved calcination procedure, during which boron is kept in a stable tetrahedral/saturated coordination and boron hydrolysis and extraction as well as T-atom reorganizations are avoided. Framework boron can be extracted from the calcined boron MFI material by refluxing in aqueous hydrochloric acid (pH <- 5), leaving thermally stable (up to 400°C, N 2 ) homogeneously distributed silanol nests, which are useful reactive sites for postsynthesis reoccupation." @default.
- W2149304866 created "2016-06-24" @default.
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- W2149304866 date "1993-02-01" @default.
- W2149304866 modified "2023-10-13" @default.
- W2149304866 title "Calcination and deboronation of [B]-MFI single crystals" @default.
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- W2149304866 doi "https://doi.org/10.1016/0144-2449(93)90072-b" @default.
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