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- W2149382279 abstract "Abstract Microwave-assisted oxidative rearrangement of 3′-iodotetraalkoxychalcones with hypervalent iodine such as [hydroxy(tosyloxy)iodo]benzene or [bis(trifluoroacetoxy)iodo]benzene, followed by microwave-mediated hydrolysis and in situ cyclization of the resultant acetals gave 6-iodotrialkoxyisoflavones. Pd(0)-catalyzed coupling reaction of the 6-iodoisoflavones with 2-methyl-3-butyn-2-ol under microwave irradiation gave 6-alkynylisoflavones, whose hydrogenation gave the respective hydrates of wighteone, lupisoflavone and derrubone. Wighteone ( 1a ), lupisoflavone ( 1b ) and derrubone ( 1c ) were obtained by dehydration of their respective hydrates under microwave irradiation." @default.
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- W2149382279 date "2007-01-02" @default.
- W2149382279 modified "2023-09-24" @default.
- W2149382279 title "Microwave-Assisted Regioselective Synthesis of Natural 6-Prenylpolyhydroxyisoflavones and Their Hydrates with Hypervalent Iodine Reagents." @default.
- W2149382279 cites W2950630548 @default.
- W2149382279 doi "https://doi.org/10.1002/chin.200701220" @default.
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