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- W2149530300 abstract "Heterocycle containing nitroaromatics were reduced by Mo(CO)6 and DBU in EtOH under microwave irradiation within 15 min. Under the same conditions, 4-fluoronitrobenzene was reduced to 4-fluoroaniline, whereas 2-chloro-1-fluoro-4-nitrobenzene afforded a mixture of 3-chloro-4-fluoroaniline and 3-chloro-4-ethoxyaniline. The extent of the competing SNAr/reduction process could be influenced by the nature of the solvent, with t-BuOH the inert solvent of choice. The latter was used as solvent for SNAr/reductions of 2-chloro-1-fluoro-4-nitrobenzene with S-nucleophiles to yield 3-chloro-4-mercaptoanilines." @default.
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- W2149530300 date "2008-10-01" @default.
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- W2149530300 title "Microwave mediated reduction of heterocycle and fluorine containing nitroaromatics with Mo(CO)6 and DBU" @default.
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- W2149530300 doi "https://doi.org/10.1016/j.tet.2008.08.036" @default.
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