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• W2149659162 abstract "Samples prepared following dissolution dynamic nuclear polarization (DNP) enable the detection of NMR spectra from low-γ nuclei with outstanding sensitivity, yet have limited use for the enhancement of abundant species like (1)H nuclei. Small- and intermediate-sized molecules, however, show strong heteronuclear cross-relaxation effects: spontaneous processes with an inherent isotopic selectivity, whereby only the (13)C-bonded protons receive a polarization enhancement. These effects are here combined with a recently developed method that delivers homonuclear-decoupled (1)H spectra in natural abundance samples based on heteronuclear couplings to these same, (13)C-bonded nuclei. This results in the HyperBIRD methodology; a single-shot combination of these two effects that can simultaneously simplify and resolve complex, congested (1)H NMR spectra with many overlapping spin multiplets, while achieving 50-100 times sensitivity enhancements over conventional thermal counterparts." @default.
• W2149659162 created "2016-06-24" @default.
• W2149659162 creator A5071742208 @default.
• W2149659162 creator A5072340391 @default.
• W2149659162 date "2014-09-26" @default.
• W2149659162 modified "2023-10-07" @default.
• W2149659162 title "HyperBIRD: A Sensitivity‐Enhanced Approach to Collecting Homonuclear‐Decoupled Proton NMR Spectra" @default.
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• W2149659162 doi "https://doi.org/10.1002/anie.201407869" @default.
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