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- W2149849785 abstract "It is of great importance in the pharmaceutical fields to discover, produce, and isolate crystalline polymorphs of a given solid drug and to control their polymorphic transformations. In this paper, we report that a cyclic oligosaccharide derivative, 2,6-di-O-methyl-β-cyclodextrin, is useful for detection and isolation of Ostwald's intermediate metastable polymorphs occurring during an early stage of crystallization. The metastable Form IV of a hyperglycemic agent, tolbutamide, exclusively crystallized from an aqueous solution of 2,6-di-O-methyl-β-cyclodextrin, whereas the stable Form I crystallized in the absence of the cyclodextrin. The selective crystallization of the metastable Form IV was attributable to an inhibition of the solution-mediated transformation of the metastable form to the stable form by the complexation with 2,6-di-O-methyl-β-cyclodextrin." @default.
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- W2149849785 date "2006-03-29" @default.
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- W2149849785 title "Selective Crystallization of the Metastable Form IV Polymorph of Tolbutamide in the Presence of 2,6-Di-<i>O</i>-methyl-β-cyclodextrin in Aqueous Solution" @default.
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- W2149849785 doi "https://doi.org/10.1021/cg060001o" @default.
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