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- W2150018712 abstract "Abstract The reaction of azulenes with several sulfoxides in the presence of acid anhydrides to afford the corresponding 1‐azulenylsulfonium and 1,3‐azulenediyldisulfonium ions is reported. The subsequent conversion of these ions in high yields into 1‐azulenyl methyl and phenyl sulfides and 1,3‐bis(methyl‐ and phenylthio)azulenes through treatment with diethylamine is also described. Reaction of the 1‐azulenyl sulfides with MCPBA afforded 1‐azulenyl sulfoxides, which were then efficiently transformed into 1,1′‐biazulene derivatives under acidic conditions. The redox properties of 1‐azulenyl methyl and phenyl sulfides, 1,3‐bis(methyl‐ and phenylthio)azulenes, and 1,1′‐biazulene derivatives bearing methylthio or phenylthio substituents on each azulene ring are reported based on the results of cyclic voltammetry experiments.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)" @default.
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- W2150018712 date "2008-02-13" @default.
- W2150018712 modified "2023-10-07" @default.
- W2150018712 title "Synthesis and Redox Behavior of 1‐Azulenyl Sulfides and Efficient Synthesis of 1,1′‐Biazulenes" @default.
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- W2150018712 doi "https://doi.org/10.1002/ejoc.200700959" @default.
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