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- W2150241249 abstract "Abstract A novel methylcellulose‐immobilized restricted access media column with strong cation‐exchange groups on an internal surface (MC‐SCX) was evaluated for the direct injection analysis of basic polar drugs in plasma by column‐switching liquid chromatography/mass spectrometry (LC/MS). Analytical conditions, including an automated pretreatment step and MS detection, were optimized for a series of basic drugs (doxepin, desipramine, imipramine, nortriptyline, amitriptyline, clomipramine). On‐line pretreatment with the MC‐SCX column followed by fast gradient analysis using a C18 column resulted in a total analysis cycle time of 7 min for each spiked plasma sample. More than 150 plasma samples spiked with target compounds were measured without compromising MS detection (relative standard deviations less than 11% for all compounds, and regression coefficients greater than 0.99). Copyright © 2005 John Wiley & Sons, Ltd." @default.
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- W2150241249 date "2005-09-06" @default.
- W2150241249 modified "2023-10-18" @default.
- W2150241249 title "On-line pretreatment using methylcellulose-immobilized cation-exchange restricted access media for direct liquid chromatography/mass spectrometric determination of basic drugs in plasma" @default.
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- W2150241249 doi "https://doi.org/10.1002/rcm.2130" @default.
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