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- W2152803562 abstract "A series of novel heterochelates of the type [Fe(An)(L)(H2O)2]•mH2O [where H2An = 4,4′-(arylmethylene)bis(3-methyl-1-phenyl-4,5-dihydro-1H-pyrazol-5-ol); aryl = 4-nitrophenyl, m = 1 (H2A1); 4-chlorophenyl, m = 2 (H2A2); phenyl, m = 2 (H2A3); 4-hydroxyphenyl, m = 2 (H2A4); 4-methoxyphenyl, m = 2 (H2A5); 4-hydroxy-3-methoxyphenyl, m = 1.5 (H2A6); 2-nitrophenyl, m = 1.5 (H2A7); 3-nitrophenyl, m = 0.5 (H2A8); p-tolyl, m = 1 (H2A9) and HL = 1-cyclopropyl-6-fluoro-4-oxo-7-(piperazin-1-yl)-1,4-dihydroquinoline-3-carboxylic acid] were investigated. They were characterized by elemental analysis (FT-IR, 1H- & 13C-NMR, and electronic) spectra, magnetic measurements and thermal studies. The FAB-mass spectrum of [Fe(A3)(L)(H2O)2]•2H2O was determined. Magnetic moment and reflectance spectral studies revealed that an octahedral geometry could be assigned to all the prepared heterochelates. Ligands (H2An) and their heterochelates were screened for their in-vitro antibacterial activity against Bacillus subtilis, Staphylococcus aureus, Escherichia coli and Serratia marcescens bacterial strains. The kinetic parameters such as order of reaction (n), the energy of activation (Ea), the pre-exponential factor (A), the activation entropy (ΔS#), the activation enthalpy (ΔH#) and the free energy of activation (ΔG#) are reported. Copyright © 2009 John Wiley & Sons, Ltd." @default.
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- W2152803562 date "2009-01-01" @default.
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- W2152803562 title "Novel drug-based Fe(III) heterochelates: synthetic, spectroscopic, thermal andin-vitroantibacterial significance" @default.
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- W2152803562 doi "https://doi.org/10.1002/aoc.1581" @default.
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