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• W2152996936 startingPage "1242" @default.
• W2152996936 abstract "The ceramic precursor for ZrC/SiC was prepared via solution‐based processing using polyzirconoxane, polycarbosilane, and divinylbenzene. The precursor could be transformed into ZrC/SiC ceramic powders at relative low temperature (1500°C). The cross‐linking process of precursor was studied by FT – IR . The conversion from precursor into ceramic was investigated by TGA , XRD . The ceramic compositions and microstructures were identified by element analysis, Raman spectra, SEM , and corresponding EDS . The results indicated that the ceramic samples remained amorphous below 1000°C and t–ZrO 2 initially generated at 1200°C. Further heating to 1400°C led to the formation of ZrC and SiC with the phase transformation of ZrO 2 and almost pure ZrC/SiC could be obtained upon heat‐treatment at 1500°C. During heat treatments, the ceramic sample changed from compact to porous due to carbothermal reduction. The ceramic powders with particle size of 100 nm~400 nm consisted of high crystalline degree ZrC and SiC phases, and Zr, Si, C were well distributed at the different sites in ceramic powders. The free carbon content was lowered to 1.60 wt% in final ZrC/SiC composite ceramics." @default.
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• W2152996936 date "2014-03-14" @default.
• W2152996936 modified "2023-10-18" @default.
• W2152996936 title "Synthesis, Characterization, and Microstructure of ZrC/SiC Composite Ceramics via Liquid Precursor Conversion Method" @default.
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• W2152996936 doi "https://doi.org/10.1111/jace.12876" @default.
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