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- W2153934103 abstract "Four D‐altritol nucleosides with a 3′‐O‐tert‐butyldimethylsilyl protecting group are synthesized (base moieties are adenine, guanine, thymine and 5‐methylcytosine). The nucleosides are obtained by ring opening reaction of 1,5:2,3‐dianhydro‐4,6‐O‐benzylidene‐D‐allitol. Optimal reaction circumstances (NaH, LiH, DBU, phase transfer, microwave irridation) for the introduction of the heterocycles are base‐specific. For the introduction of the 3′‐O‐silyl protecting group, long reaction times and several equivalents of tert‐butyldimethylsilyl chloride are needed." @default.
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- W2153934103 date "2004-01-01" @default.
- W2153934103 modified "2023-09-23" @default.
- W2153934103 title "Synthesis of D‐Altritol Nucleosides with a 3′‐<i>O‐Tert</i>‐Butyldimethylsilyl Protecting Group" @default.
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- W2153934103 doi "https://doi.org/10.1081/ncn-120028338" @default.
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