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• W2154608276 abstract "Abstract In the reactions of perfluorinated 1-methyl- (2) and 1-ethyl-benzocyclobutene (3) with bromine in an SbF5 medium, cleavage of the four-membered ring of the starting compounds giving 2-bromoperfluoroisopropylbenzene (8) and 2-bromoperfluoro-sec-butylbenzene (9), respectively, was observed. In the system Br2SbF5, perfluorinated 1,1- (4) and 1,2-diethylbenzocyclobutene (5) undergo bromofluorination of the aromatic ring and breaking of the C1C2 bond of the four-membered ring. Thus, in the Br2SbF5 system, compound 5 gives 4-bromoperfluoro-1,2-dipropylcyclohexene (10) and perfluoro-1,2-dipropylcyclohexene (11), and isomer 4 gives perfluoro-1,1-diethyl-3,4,5,6-tetrahydrobenzocyclobutene (15) and perfluoro-1-methyl-2-(pent-2-ene-3-yl)cyclohexene (16). The latter is obtained by heating compound 15 with SbF5 or CsF." @default.
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• W2154608276 date "1996-04-01" @default.
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• W2154608276 title "The alicyclic ring cleavage and other transformations of perfluorinated 1-alkyl-, 1,1- and 1,2-dialkyl-benzocyclobutenes in the system Br2SbF5" @default.
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• W2154608276 doi "https://doi.org/10.1016/0022-1139(96)03390-8" @default.
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