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• W2154901441 abstract "Dimeres Dimethylgallium-bis(trimethylsilyl)phosphan, [Me2GaP(SiMe3)2]2 (Me = CH3), wird aus Me2GaCl und P(SiMe3)3 in heißem Toluol synthetisiert. Die Verbindung kristallisiert in der triklinen Raumgruppe P1 mit den Gitterkonstanten a = 909,8(2), b = 960,5(2), c = 971,6(2) pm; α = 76,75(1)°, β = 80,35(1)°, γ = 63,94(1)° und Z = 1 (Dimer). Die GaP-Abstände des planaren Ga2P2-Gerüsts betragen 244,8 und 245,2 pm, die Ringwinkel 91,8° (GaPGa) bzw. 88,2° (PGaP). Das Schwingungsspektrum (IR und Raman des Feststoffs) wurde aufgenommen und zugeordnet, für das Molekülskelett [C2GaP(SiC3)2]2 werden mit dem PC-Programm von Fleischhauer [26] Kraftkonstantenrechnungen durchgeführt. Dimethylgallium-bis(trimethylsilyl)phosphane, Vibrational Spectrum, Force Constants, and X-Ray Structure Dimeric dimethylgallium-bis(trimethylsilyl)phosphane, [Me2GaP(SiMe3)2]2, (Me = CH3) is synthesized from Me2GaCl and P(SiMe3)3 in hot toluene. The compound crystallizes in the triclinic space group P1 with the cell parameters a = 909.8(2), b = 960.5(2), c = 971.6(2) pm; α = 76.75(1)°, β = 80.35(1)°, γ = 63.94(1)° and Z = 1 (dimer). The GaP distances are 244.8 and 245.2 pm, the ring angles are 91.8° (GaPGa) and 88.2° (PGaP), respectively. The vibrational spectrum (IR and Raman for the solid) has been measured and assigned; force constants calculations are carried out for the skeleton [C2GaP(SiC3)2]2 using Fleischhauers [26] PC-program." @default.
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• W2154901441 date "1995-08-01" @default.
• W2154901441 modified "2023-10-14" @default.
• W2154901441 title "Dimethylgallium-bis(trimethylsilyl)phosphan Schwingungsspektrum, Kraftkonstanten und Struktur" @default.
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• W2154901441 doi "https://doi.org/10.1002/zaac.19956210813" @default.
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