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• W2155023126 abstract "Chalcopyrite α-CuInSe2 (α-CIS) was prepared from mixed powders of Cu2Se and In2Se3 by annealing in the Se- and the non-Se environments. The mechanically ground powders were in an overall amorphous state. The mechanical alloying produced Cu3Se2 and CuSe compounds. At relatively low temperature, Cu3Se2 decomposed, Cu2−xSe and CuSe formed. The reaction for the formation of α-CuInSe2 occurred essentially at a temperature at ∼350 °C in both the Se- and the non-Se environments. In the non-Se environment, reactions occurred by a solid–solid reaction and a certain amount of Se were released from the mixed powder, resulting in poor crystalline α-CuInSe2 powders. When annealed in the Se environment, low-melting Se-rich Cu-Se compounds were produced during reaction. The reactions occurred by a liquid–solid reaction above 450 °C. Large-grained and good crystalline quality of chalcopyrite CIS with near stoichiometric atomic ratio was obtained above 450 °C." @default.
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• W2155023126 date "2011-06-24" @default.
• W2155023126 modified "2023-09-27" @default.
• W2155023126 title "Formation of CuInSe2 from Cu2Se and In2Se3 compounds" @default.
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• W2155023126 doi "https://doi.org/10.1002/pssa.201127206" @default.
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