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- W2156868575 abstract "Abstract A new strategy for the one‐pot preparation of ABA‐type block‐graft copolymers via a combination of Cu‐catalyzed azide‐alkyne cycloaddition (CuAAC) “click” chemistry with atom transfer nitroxide radical coupling (ATNRC) reaction was reported. First, sequential ring‐opening polymerization of 4‐glycidyloxy‐2,2,6,6‐tetramethylpiperidine‐1‐oxyl (GTEMPO) and 1‐ethoxyethyl glycidyl ether provided a backbone with pendant TEMPO and ethoxyethyl‐protected hydroxyl groups, the hydroxyl groups could be recovered by hydrolysis and then esterified with 2‐bromoisobutyryl bromide, the bromide groups were converted into azide groups via treatment with NaN 3 . Subsequently, bromine‐containing poly( tert ‐butyl acrylate) (P t BA‐Br) was synthesized by atom transfer radical polymerization. Alkyne‐containing polystyrene (PS‐alkyne) was prepared by capping polystyryl‐lithium with ethylene oxide and subsequent modification by propargyl bromide. Finally, the CuAAC and ATNRC reaction proceeded simultaneously between backbone and P t BA‐Br, PS‐alkyne. The effects of catalyst systems on one‐pot reaction were discussed. The block‐graft copolymers and intermediates were characterized by size‐exclusion chromatography, 1 H NMR, and FT‐IR in detail. © 2010 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem, 2010" @default.
- W2156868575 created "2016-06-24" @default.
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- W2156868575 date "2010-10-13" @default.
- W2156868575 modified "2023-10-18" @default.
- W2156868575 title "One-pot preparation of ABA-type block-graft copolymers via a combination of “click” chemistry with atom transfer nitroxide radical coupling reaction" @default.
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- W2156868575 doi "https://doi.org/10.1002/pola.24349" @default.
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