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- W2157172318 abstract "n-Octadecyl S-methyl xanthate, m.p. 38–39°, and n-hexadecyl S-methyl xanthate, m.p. 28–28.5°, were prepared for the first time, and were used to study the behavior of the S-methyl xanthate group toward reagents commonly used in research on carbohydrates. Although stable to some conditions of acetylation, hydrolysis, and methanolysis, the S-methyl xanthate group was destroyed by all methylating agents tried, with the exception of nitrosomethylurethane. The latter reagent converted a sodium xanthate salt in high yield to the S-methyl ester. Octadecyl and hexadecyl S-methyl xanthates when oxidized with hydrogen peroxide yielded crystalline substances of composition C 20 H 40 O 4 S 2 and C 18 H 36 O 4 S 2 , respectively, whose structures were not determined. These substances each contained three additional oxygen atoms. Various attempts to estimate the S-methyl xanthate group by oxidation with bromine or periodic acid, or by reduction to methyl iodide, were unsuccessful." @default.
- W2157172318 created "2016-06-24" @default.
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- W2157172318 date "1956-09-01" @default.
- W2157172318 modified "2023-09-25" @default.
- W2157172318 title "THE CHEMICAL STABILITY OF THE S-METHYL XANTHATES OF SOME SIMPLE ALCOHOLS" @default.
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- W2157172318 doi "https://doi.org/10.1139/v56-167" @default.
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