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- W2157818323 abstract "Abstract A new and efficient strategy was developed for the preparation of 1,2,4-trimethoxybenzene (3, a powerful attractant of Euglossini bees) and its C-3 derivatives (7a–j), from vanillin (2) in 56% overall yield. Keywords: Aromatic lithiationdirected metalationEuglossini beesregioselectivity1,2,4-trimethoxybenzene ACKNOWLEDGMENTS We thank CAPES, CNPQ, FAPERJ, and FUJB for financial support and also Qiang Wang, a Postdoctoral student in Clayton H. Heathcock's research group, Department of Chemistry, University of California Berkeley, USA, for personal contributions. Notes ∗There were employed 1,1,eq of the organolithium reagent and CH3I. ∗∗Time of the reaction before the addition of the electrophile." @default.
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- W2157818323 date "2009-09-18" @default.
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- W2157818323 title "Synthesis of 1,2,4-Trimethoxybenzene and Its Selective Functionalization at C-3 by Directed Metalation" @default.
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