Matches in SemOpenAlex for { <https://semopenalex.org/work/W2158404797> ?p ?o ?g. }
Showing items 1 to 88 of
88
with 100 items per page.
- W2158404797 endingPage "87" @default.
- W2158404797 startingPage "84" @default.
- W2158404797 abstract "A universal peroxyoxalate-chemiluminescence detection system for high performance liquid chromatography, available for a variety of mobile phases, has been developed. The system consisted of a dual-head short-stroke pump and a chemiluminescence detector. The standard conditions using bis(2,4,6-trichlorophenyl) oxalate (TCPO) as aryl oxalate were as follows. The first postcolumn solution was the mixture of 0.5 M imidazole-nitric acid (pH 7.5) and acetonitrile (1:4, v/v). The second was acetonitrile containing TCPO-hydrogen peroxide. These two solutions were delivered by the two pump-heads. After the pH of the column eluate was adjusted to the optimum range (6.5-7.5) by the first postcolumn solution, the solution was mixed with the second postcolumn solution. After flowing through a reaction coil, the chemiluminescence of the mixture was monitored. Using this system, a high sensitivity (fmol level) was obtained for perylene as an analyte with mobile phases having different pH values (2.0-8.0). Polycyclic aromatic hydrocarbons became detectable to a high sensitivity even after the column separation using an acidic mobile phase. The detection sensitivity of nitrated pyrenes after on-line electrochemical reduction using an acidic mobile phase was also increased. This system might be available for other aryl oxalates by some modifications of the postcolumn solutions." @default.
- W2158404797 created "2016-06-24" @default.
- W2158404797 creator A5013040020 @default.
- W2158404797 creator A5017613243 @default.
- W2158404797 creator A5037409124 @default.
- W2158404797 creator A5048823673 @default.
- W2158404797 creator A5080574833 @default.
- W2158404797 date "1992-03-01" @default.
- W2158404797 modified "2023-09-26" @default.
- W2158404797 title "A universal peroxyoxalate-chemiluminescence detection system for mobile phases of differing pH" @default.
- W2158404797 cites W1984775127 @default.
- W2158404797 cites W1988176781 @default.
- W2158404797 cites W2005969746 @default.
- W2158404797 cites W2011068306 @default.
- W2158404797 cites W2011420488 @default.
- W2158404797 cites W2016521532 @default.
- W2158404797 cites W2021960589 @default.
- W2158404797 cites W2025776458 @default.
- W2158404797 cites W2026173562 @default.
- W2158404797 cites W2048233010 @default.
- W2158404797 cites W2055441147 @default.
- W2158404797 cites W2055976065 @default.
- W2158404797 cites W2058321799 @default.
- W2158404797 cites W2058699918 @default.
- W2158404797 cites W2067980898 @default.
- W2158404797 cites W2069250445 @default.
- W2158404797 cites W2089126087 @default.
- W2158404797 cites W2091142348 @default.
- W2158404797 cites W2092059619 @default.
- W2158404797 cites W2136135718 @default.
- W2158404797 cites W2138660958 @default.
- W2158404797 doi "https://doi.org/10.1002/bmc.1130060208" @default.
- W2158404797 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/1638095" @default.
- W2158404797 hasPublicationYear "1992" @default.
- W2158404797 type Work @default.
- W2158404797 sameAs 2158404797 @default.
- W2158404797 citedByCount "7" @default.
- W2158404797 countsByYear W21584047972012 @default.
- W2158404797 crossrefType "journal-article" @default.
- W2158404797 hasAuthorship W2158404797A5013040020 @default.
- W2158404797 hasAuthorship W2158404797A5017613243 @default.
- W2158404797 hasAuthorship W2158404797A5037409124 @default.
- W2158404797 hasAuthorship W2158404797A5048823673 @default.
- W2158404797 hasAuthorship W2158404797A5080574833 @default.
- W2158404797 hasConcept C11445154 @default.
- W2158404797 hasConcept C119128265 @default.
- W2158404797 hasConcept C145802702 @default.
- W2158404797 hasConcept C178790620 @default.
- W2158404797 hasConcept C179104552 @default.
- W2158404797 hasConcept C185592680 @default.
- W2158404797 hasConcept C2776351790 @default.
- W2158404797 hasConcept C2777463227 @default.
- W2158404797 hasConcept C43617362 @default.
- W2158404797 hasConcept C533411734 @default.
- W2158404797 hasConcept C73826308 @default.
- W2158404797 hasConceptScore W2158404797C11445154 @default.
- W2158404797 hasConceptScore W2158404797C119128265 @default.
- W2158404797 hasConceptScore W2158404797C145802702 @default.
- W2158404797 hasConceptScore W2158404797C178790620 @default.
- W2158404797 hasConceptScore W2158404797C179104552 @default.
- W2158404797 hasConceptScore W2158404797C185592680 @default.
- W2158404797 hasConceptScore W2158404797C2776351790 @default.
- W2158404797 hasConceptScore W2158404797C2777463227 @default.
- W2158404797 hasConceptScore W2158404797C43617362 @default.
- W2158404797 hasConceptScore W2158404797C533411734 @default.
- W2158404797 hasConceptScore W2158404797C73826308 @default.
- W2158404797 hasIssue "2" @default.
- W2158404797 hasLocation W21584047971 @default.
- W2158404797 hasLocation W21584047972 @default.
- W2158404797 hasOpenAccess W2158404797 @default.
- W2158404797 hasPrimaryLocation W21584047971 @default.
- W2158404797 hasRelatedWork W1999601188 @default.
- W2158404797 hasRelatedWork W2003483767 @default.
- W2158404797 hasRelatedWork W2005437743 @default.
- W2158404797 hasRelatedWork W2054471285 @default.
- W2158404797 hasRelatedWork W2057575498 @default.
- W2158404797 hasRelatedWork W2064757938 @default.
- W2158404797 hasRelatedWork W2080424545 @default.
- W2158404797 hasRelatedWork W2090162036 @default.
- W2158404797 hasRelatedWork W2130182718 @default.
- W2158404797 hasRelatedWork W4230939517 @default.
- W2158404797 hasVolume "6" @default.
- W2158404797 isParatext "false" @default.
- W2158404797 isRetracted "false" @default.
- W2158404797 magId "2158404797" @default.
- W2158404797 workType "article" @default.