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• W2158851540 abstract "A microwave-assisted carbothermal reduction and nitridation (CTR/N) method has been used for successful preparation of monophasic β′-SiAlON starting from kaolinite and carbon black. Phase pure β′-SiAlON has been obtained in under 60 min in microwave field. The z value of microwave prepared β′-SiAlON is found to be 2.95, which is very close to the expected value from kaolinite composition. Formation of β′-SiAlON has been monitored with XRD and MASNMR of 29Si and 27Al; the possible reaction mechanism has been discussed. Kaolinite to β′-SiAlON conversion appears to be a very rapid single-step reaction under microwave irradiation. β′-SiAlON powders have been microwave sintered to 98.7% of theoretical density in 30 min." @default.
• W2158851540 created "2016-06-24" @default.
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• W2158851540 date "2003-03-01" @default.
• W2158851540 modified "2023-10-14" @default.
• W2158851540 title "A microwave method for the preparation and sintering of β′-SiAlON" @default.
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• W2158851540 doi "https://doi.org/10.1016/s0025-5408(02)01071-1" @default.
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