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- W2158891007 abstract "Abstract By following a new synthetic approach, which is based on the in situ formation of a basic medium by the reaction between the strong base Sb(V)S 4 3− and the weak acid H 2 O, it was possible to prepare three layered thioantimonate(III) compounds of composition [TM(2,2′‐bipyridine) 3 ][Sb 6 S 10 ] (TM=Ni, Fe) and [Ni(4,4′‐dimethyl‐2,2′‐bipyridine) 3 ][Sb 6 S 10 ] under hydrothermal conditions featuring two different thioantimonate(III) network topologies. The antimony source, Na 3 SbS 4 ⋅ 9 H 2 O, undergoes several decomposition reactions and produces the Sb III S 3 species, which condenses to generate the layered anion. The application of transition‐metal complexes avoids crystallization of dense phases. The reactions are very fast compared to conventional hydrothermal/solvothermal syntheses and are much less sensitive to changes of the reaction parameters." @default.
- W2158891007 created "2016-06-24" @default.
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- W2158891007 date "2014-10-21" @default.
- W2158891007 modified "2023-10-18" @default.
- W2158891007 title "A Strategy for the Preparation of Thioantimonates Based on the Concept of Weak Acids and Corresponding Strong Bases" @default.
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- W2158891007 doi "https://doi.org/10.1002/chem.201404396" @default.
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