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• W2160577110 startingPage "11010" @default.
• W2160577110 abstract "Diarylmethylamines are key intermediates and products in the pharmaceutical industry. Herein we disclose a novel method toward the synthesis of these important compounds via CH functionalization. Presented is a reversible deprotonation of N-Boc benzylalkylamines at the benzylic CH with in situ arylation by a NiXantPhos-based palladium catalyst (50-93 % yield, 29 examples). The method is also successful with N-Boc-tetrahydroisoquinolines. The advantages of this method are it avoids strong bases, low temperatures, and the need to transmetallate to main group metals for the coupling." @default.
• W2160577110 created "2016-06-24" @default.
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• W2160577110 date "2015-06-30" @default.
• W2160577110 modified "2023-10-18" @default.
• W2160577110 title "Palladium-Catalyzed C(sp³)H Arylation of<i>N</i>-Boc Benzylalkylamines via a Deprotonative Cross-Coupling Process" @default.
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• W2160577110 doi "https://doi.org/10.1002/chem.201502017" @default.
• W2160577110 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/5079650" @default.
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• W2160577110 hasPublicationYear "2015" @default.
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