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• W2161899549 abstract "Silicon carbide hot-pressed with aluminum, boron, and carbon as sintering aids (ABC–SiC), was studied by transmission electron microscopy. Both grain-boundary films and inclusions were prevalent in this material. The present study characterized the inclusions located in triple-junctions, grain boundaries, and the interior of the SiC grains, with emphases on phases not scrutinized before. These inclusions were crystalline, in contrast to the amorphous grain-boundary films. Two dominant types of boron-free triple-junction phases containing Al(Si)-O-C-(S) and Al(Si)-O were identified, where sulfur was an unexpected contaminant, and silicon came from SiO2 or from dissolution of SiC. Boron-containing inclusions with a composition Al-O-B-C were frequently observed inside SiC grains. Although the boron-free aluminum-rich phases wet the grain boundaries completely and are, therefore, effective sintering additives, the boron-containing Al(Si)-O-B-C did not wet the grain boundaries. The structure and chemical composition of these boron-containing intragranular inclusions were determined, and their mechanism of formation is discussed." @default.
• W2161899549 created "2016-06-24" @default.
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• W2161899549 date "2001-04-01" @default.
• W2161899549 modified "2023-10-12" @default.
• W2161899549 title "Secondary Phases in Hot-Pressed Aluminum-Boron-Carbon?Silicon Carbide" @default.
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• W2161899549 doi "https://doi.org/10.1111/j.1151-2916.2001.tb00746.x" @default.
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